814 USB Sample Processor Manual 8.814.
Metrohm AG CH-9101 Herisau Switzerland Phone +41 71 353 85 85 Fax +41 71 353 89 01 info@metrohm.com www.metrohm.com 814 USB Sample Processor Manual 8.814.
Teachware Metrohm AG CH-9101 Herisau teachware@metrohm.com This documentation is protected by copyright. All rights reserved. Although all the information given in this documentation has been checked with great care, errors cannot be entirely excluded. Should you notice any mistakes please send us your comments using the address given above. Documentation in additional languages can be found on http://products.metrohm.com under Literature/Technical documentation.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents Table of contents 1 Introduction 1.1 1 The 814 USB Sample Processor in the Titrando system ......................................................................................... 1 1.2 Instrument description ......................................................... 2 1.2.1 Model versions ........................................................................ 2 1.2.2 Instrument components .......................................................... 4 1.2.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents 3.9 Connecting USB devices ..................................................... 30 3.9.1 Connecting a barcode reader ................................................. 30 3.10 Mounting the drip pan ....................................................... 31 3.11 Attaching the sample rack ................................................. 32 3.12 Mounting the safety shield ................................................ 32 4 Handling and maintenance 34 4.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents 9 Accessories Index 814 USB Sample Processor 47 9.1 Scope of delivery 814 USB Sample Processor 2.814.0010 .......................................................................... 47 9.2 Scope of delivery 814 USB Sample Processor 2.814.0020 .......................................................................... 52 9.3 Scope of delivery 814 USB Sample Processor 2.814.0030 .......................................................................... 58 9.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures Table of figures Figure 1 Figure 2 Figure 3 Figure 4 Figure 5 Figure 6 Figure 7 Figure 8 Figure 9 Figure 10 Figure 11 Figure 12 Figure 13 Figure 14 Figure 15 Figure 16 Figure 17 Figure 18 Figure 19 Figure 20 Figure 21 Figure 22 Figure 23 Figure 24 Figure 25 Figure 26 Figure 27 Figure 28 Figure 29 Figure 30 VI ￭￭￭￭￭￭￭￭ The Titrando system .......................................................................... 1 Front 814 USB Sample Processor ....................
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction 1 Introduction 1.1 The 814 USB Sample Processor in the Titrando system The 814 USB Sample Processor is a component of the modular Titrando system. Operation is carried out by a Touch Control with touch-sensitive screen ("Stand alone" titrator) or by a computer with a corresponding software. A Titrando system can contain numerous, various kinds of devices.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1.2 Instrument description Up to three control devices (Titrandos, Dosing Interfaces, USB Sample Processors etc.) can be controlled via USB connection by the Touch Control. With the tiamo software the system can arbitrarily be extended with control devices. Updating the device software is described in the manual for the Touch Control or in the tiamo help, respectively. 1.2 Instrument description The 814 USB Sample Processor is a versatile instrument.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction 2.814.0010 1-Tower version ￭ ￭ ￭ ￭ ￭ ￭ ￭ 1 membrane pumpe and 1 valve 1 connector for an external pump 1 stirrer connector (tower stirrer) 1 Swing Head connector 3 MSB connectors for dosing devices or stirrers 2 USB connectors 1 controller connection 2.814.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1.2 Instrument description 2.814.0120 2-Tower version ￭ ￭ ￭ ￭ ￭ ￭ 4 membrane pumps and 4 valves 2 stirrer connectors (tower stirrer) 2 Swing Head connectors 3 MSB connectors for dosing devices or stirrers 2 USB connectors 1 controller connection 2.814.0130 2-Tower version ￭ ￭ ￭ ￭ ￭ ￭ 1.2.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1.2.3 1 Introduction Intended use The 814 USB Sample Processor is designed for usage as an automation system in analytical laboratories. It is not suitable for usage in biochemical, biological or medical environments in its basic equipment version. The present instrument is suitable for processing chemicals and flammable samples.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1.4 Safety instructions Warning This symbol draws attention to a possible biological hazard. Caution This symbol draws attention to a possible damage of instruments or instrument parts. Note This symbol marks additional information and tips. 1.4 Safety instructions 1.4.1 General notes on safety Warning This instrument may only be operated in accordance with the specifications in this documentation.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction Mains voltage Warning An incorrect mains voltage can damage the instrument. Only operate this instrument with a mains voltage specified for it (see rear panel of the instrument). Protection against electrostatic charges Warning Electronic components are sensitive to electrostatic charges and can be destroyed by discharges.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1.4 Safety instructions Warning Always install the safety shield supplied with the equipment before using the instrument for the first time. Pre-installed safety shields are not allowed to be removed. The 814 USB Sample Processor may not be operated without a safety shield! Warning Personnel are not permitted to reach into the working area of the instrument while operations are running! A considerable risk of injury exists for the user.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1.4.5 1 Introduction Flammable solvents and chemicals Warning All relevant safety measures are to be observed when working with flammable solvents and chemicals. ￭ ￭ ￭ ￭ 1.4.6 Set up the instrument in a well-ventilated location. Keep all sources of flame far from the workplace. Clean up spilled liquids and solids immediately. Follow the safety instructions of the chemical manufacturer.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 2.1 Front and rear 2 Overview of the instrument 2.1 Front and rear 4 1 5 2 6 7 3 Figure 2 Front 814 USB Sample Processor 1 Safety shield (6.2751.080) other models, see chap. Accessories. 2 Sample rack (6.2041.310) other models, see chap. Accessories. 3 Stirrer rail For magnetic stirrer (741 Stirrer). 4 Guide chain For cables and tubings. 5 Lift With titration head holder. 6 Beaker sensor 7 Turntable With guide bolts.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 2 Overview of the instrument 1 8 T2 T1 2 3 4 5 6 USB 2 7 Figure 3 Rear 814 USB Sample Processor 1 Distributor For rinsing equipment. 2 Membrane pump Pump 1. 3 Pump connection Pump 2. For the external pump. 4 Pump valve 5 Swing Head connector Mini DIN socket (9-pin). 6 Stirrer connector DIN socket. For rod stirrer (802 Stirrer) or magnetic stirrer (741 Stirrer). 7 Rear panel with connectors 8 Warning symbol (see Chapter 1.4.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 2.2 Rear panel Rear panel 1 2 WARNING - Fire Hazard - 3 with the same type and rating of fuse U: 100 - 240 V 5 f: 50 - 60 Hz Made by Metrohm Herisau Switzerland USB 2 Figure 4 P: 115W MSB 1 For continued protection replace only USB 1 4 Contr. MSB 2 MSB 3 Nr. 2.2 Connector strip 1 USB connectors 2 Controller connector For the connection to the PC or Touch Control. 3 MSB connector For stirrers, dosing devices, Remote Box.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 2 Overview of the instrument Magnet codes Every single sample rack can be unambiguously identified by means of a magnet code. The Sample Processor can thus recognize automatically which rack is in place. When replacing a rack, this should first be returned to starting position using the Rack initialization function (see "Manual Control" in the control software). This will enable an unambiguous recognition of the rack and thus the correct positioning of the beaker.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.1 Setting up the instrument 3 Installation 3.1 Setting up the instrument 3.1.1 Packaging The instrument is supplied in highly protective special packaging together with the separately packed accessories. Keep this packaging, as only this ensures safe transportation of the instrument. 3.1.2 Checks Immediately after receipt, check whether the shipment has arrived complete and without damage by comparing it with the delivery note. 3.1.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.3 3 Installation Connecting a computer The 814 USB Sample Processor requires a USB connection to a computer in order to be able to be controlled by a PC software. When a 6.2151.000 controller cable is used, the instrument can be connected directly, either to a USB socket on a computer, to a connected USB hub or to a different Metrohm control instrument.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.4 Installing rinsing and aspiration equipment For Windows Vista: The instrument is recognized and the installation assistant for the driver is started automatically. Select the option "Find and install driver software". Agree to all subsequent requests. The installation assistant will be exited automatically. Note The plug on the instrument end of the 6.2151.000 controller cable is protected with an anti-pull device to prevent the cable from being pulled out accidentally.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation 6.1805.510 6.1805.420 1 2 6.1808.170 3 4 6.1812.000 Figure 8 Mounting the rinsing and aspiration tubings 1 Mount the rinsing tubings ￭ Manually tighten the three 6.1805.420 FEP tubings (48 cm) in the M6 bore holes of the distributor. Place the tubings into the guide chain (see Chapter 3.5, page 19). These are the feed lines for the spray nozzles. 2 Mount the aspiration tubing ￭ Manually tighten the 6.1805.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.4 Installing rinsing and aspiration equipment Note The opening of the tubing may need to be widened with a sharp object (e.g. with a Phillips screwdriver). A piece of sandpaper may be used to get a better grip on the tubing. Do not extend the tubing end before having slid the union nut onto the tubing. 4 Mount the outlet tubing ￭ Remove the union nut of the right-hand connector of the distributor and guide it over the end of the 6.1812.000 PTFE tubing.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation 3 Fix the rinsing tubings ￭ 3.5 Place the rinsing tubings into the guide chain. Guide chain for cables and tubing Tubings and cables can be placed into the guide chain. You can open the individual chain links with a screwdriver as follows. 1 Open the guide chain ￭ ￭ ￭ ￭ Insert a screwdriver into the groove located on the side of a chain link. Loosen the clip with a forceful leverage movement. Pull the clip out of the chain by hand.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.6 Installing the titration head Caution Take care to ensure when mounting tubing and cables that there is no traction on the drives while moving the lift or swiveling the robotic arm. This could lead to overloading of and possible damage to the drive. Remove the clips of the two lowest chain links when you install the rinsing and aspiration tubing. 3.6 Installing the titration head Mounting the titration head 6.1458.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation 6 6.0xxx.xxx 4 3 6.1236.020 5 6.1543.200 6.1543.170 1 2 2 1 6.2740.020 1 6.2709.070 Figure 12 Installing accessories for the titration 1 Insert three spray nozzles (6.2740.020) or rinsing nozzles (6.2740.030) into the oblique bore holes, see figure. 2 Insert two 6.2709.070 guide sleeves into the titration head, see figure. 3 Insert a 6.1543.200 titration tip (with antidiffusion valve) into a guide sleeve. 4 Insert a 6.1543.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.6 Installing the titration head 6 Connect a electrode cable to the electrode. Connecting the tubings In the following, the fastening of the necessary tubings is described in case rinsing and aspirating of sample vessels with the aid of integrated or external pumps is used. 6.1805.110 6.1805.510 6.1805.420 3 1 2 1 1 6.1543.200 6.1543.170 6.2740.020 Figure 13 Connecting the tubings 1 Tighten the 6.1805.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation Connecting the tower stirrer A DIN socket for connecting a rod stirrer (802 Stirrer) or a magnetic stirrer (741 Stirrer) is located on the rear side of the tower. Figure 14 Rod stirrer (802 Stirrer) Figure 15 Magnetic stirrer (741 Stirrer) Take care to observe correct orientation of the contact pins when plugging in the stirrer connection cable. The rib on the outside of the plug must match the reference mark (on the left) on the socket.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.6 Installing the titration head Insert the rod stirrer 1 2 Figure 17 802 Stirrer 6.1906.010 Insert the rod stirrer 1 Insert a propeller stirrer (802 Stirrer) from above into the opening marked with an arrow. 2 Place a stirring propeller (e.g. 6.1906.010) from below over the drive shaft of the propeller stirrer and press firmly. Installing the 741 Stirrer As alternative to a propeller stirrer, a magnetic stirrer (741 Stirrer) can be used.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation The magnetic stirrer can be moved sideways as needed. 3.7 Connecting an external pump If no integrated pump or a Sample Processor model version without pumps is used, up to two external pumps per tower can be connected. The 843 Pump Station (as model version with membrane pumps or with peristaltic pumps) has two pump drives and is connected to two sockets of the Sample Processor via the 6.2141.300 connecting cable (double cable with two plugs).
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.8 Connecting MSB devices 3.8 Connecting MSB devices In order to connect MSB devices, e.g.stirrers or dosing devices, Metrohm instruments are equipped with up a maximum of four connectors at what is referred to as the Metrohm Serial Bus (MSB). Various kinds of peripheral devices can be connected in sequence (in series, as a "daisy chain") at a single MSB connector (8-pin Mini DIN socket) and controlled simultaneously by the respective control instrument.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.8.1 3 Installation Connecting dosing devices Three dosing devices can be connected to the instrument. The types of dosing devices that are supported are: ￭ ￭ ￭ ￭ 800 Dosino 700 Dosino 805 Dosimat 685 Dosimat Warning If a Dosino is connected to the 814 USB Sample Processor then the connection cable must be equipped with a T.2400.102 ferrite core.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.8 Connecting MSB devices 3.8.2 Connecting a stirrer or titration stand You can use a magnetic stirrer 801 Stirrer or 803 Ti Stand (stirring "from below") or the 804 Ti Stand with a rod stirrer 802 Stirrer (stirring "from above"). Connect a stirrer or a titration stand as follows: 1 Connect a stirrer or titration stand ￭ ￭ ￭ ￭ Exit the control software.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.8.3 3 Installation Connecting a remote box Instruments that are controlled via remote lines and/or which send control signals via remote lines can be connected using the 6.2148.010 remote box. In addition to Metrohm, other instrument manufacturers also use similar connectors that make it possible to connect different instruments together.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.9 Connecting USB devices 3.9 Connecting USB devices Two USB connectors (Type A sockets) are available for connecting devices with USB interfaces. The 814 USB Sample Processor functions then as a USB hub (distributor). If you wish to connect more than two USB devices, you can also use an additional commercially available USB hub. Note When a USB device is connected, the control instrument recognizes which device is connected.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation Switch the barcode reader to programming mode and make the following settings: 1 ￭ ￭ ￭ ￭ ￭ 3.10 Select the keyboard layout for the desired country (USA, Germany, France, Spain, Switzerland (German)). This setting must match the setting in the control software. Make sure that the Ctrl characters (ASCII 00 to 31) are allowed to be sent. Adjust the settings so that the ASCII character 02 (STX or Ctrl B) is sent as the first character as "Preamble" or "Prefix Code".
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.11 Attaching the sample rack 3.11 Attaching the sample rack 1 Figure 25 Attaching the rack Put the rack into place as follows: 1 Carefully center the rack on the turntable. The guide bolts on the turntable must engage with the openings in the bottom of the rack. Tip: hold the rack in such a way that the printed Metrohm logo is legible horizontally. 2 Carry out the [Rack Reset] function in the manual operation of the control software. The rack is moved into starting position.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation 1 3 2 Figure 26 Mount the safety shield Proceed as follows: 1 Loosen the knurled screws on both sides of the tower. 2 Move the safety shield into position, starting from the top. Observe the corresponding illustration. 3 Fix the safety shield in place with the knurled screws. Note You can adjust the vertical position of the safety shield at any time by loosening the screws.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4.1 General 4 Handling and maintenance 4.1 General The 814 USB Sample Processor requires appropriate care. Excess contamination of the instrument may result in functional disruptions and a reduction in the service life of the sturdy mechanics and electronics of the instrument. Severe contamination can also have an influence on the measured results. Regular cleaning of exposed parts can prevent this to a large extent. Spilled chemicals and solvents must be removed immediately.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Troubleshooting 5 Troubleshooting 5.1 Sample Processor Problem Cause Remedy The instrument is not recognized by the control software. Sample Processor – No USB connection available. 1. Correctly plug in the USB connection cable on both ends. 2. Restart the control software or switch the Touch Control off and on again. Sample Processor – Power supply of the instrument is missing. 1. Plug in the mains cable on the instrument. 2.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6.1 Beaker sensor 6 Appendix 6.1 Beaker sensor Every tower of a Sample Processor is equipped with a beaker sensor detecting the availability of a sample vessel in front of the tower. An infrared sensor identifies devices of various materials if they are located in a correct position in the front of the tower. In the rack configuration of the control device or the control software, the setting 'Beaker sensor' Tower must be selected.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Appendix Figure 28 Spray nozzles - Functioning The height of the nozzles can be adjusted in the titration head in order to reach an optimal rinsing effect. 6.3 Remote interface The 6.2148.010 remote box allows devices to be controlled which cannot be connected directly to the MSB interface of the Sample Processor . 1 2 3 Figure 29 Connectors of the remote box 1 Cable For connecting the Sample Processor . 3 Remote connector For connecting devices with a remote interface.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6.3 Remote interface 6.3.1 Pin assignment of the remote interface 13 1 1 13 25 14 14 25 Figure 30 Pin assignment of the remote socket and plug The above presentation of the pin assignment of a Metrohm remote interface applies not only for the remote box, but also for all Metrohm devices with 25-pin D-Sub remote connection. Inputs +5 V approx. 50 kΩ Pull-up tp tp >20 ms active = low, inactive = high The input lines can be scanned with the SCAN command.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 814 USB Sample Processor 6 Appendix Assigment Pin No. Assigment Pin No.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 7.1 Lift and turntable 7 Technical specifications 7.1 Lift and turntable Stroke path 235 mm Maximum lift load approx. 30 N / 3 kg Lift rate adjustable, 5…25 mm/s Shift rate adjustable, 3...20 angle degrees/s 7.2 Membrane pump(s) with valve > 450 mL/min Pressure head 2 m Capacity 7.3 Interfaces and connectors Controller connection USB Upstream Port (9-pin Mini DIN socket) for connecting a computer for controlling of the instrument.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 7.4 7 Technical specifications Mains connection Voltage 100…240 V Frequency 50…60 Hz Power consumption 115 W Fuse 2.0 ATH 7.5 Safety specifications Design and testing According to EN/IEC/UL 61010-1, CSA-C22.2 No. 61010-1, EN/IEC 61010-2-081, protection class Ⅰ Safety instructions This document contains safety instructions which have to be followed by the user in order to ensure safe operation of the instrument. 7.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 7.7 Ambient temperature 7.7 Ambient temperature Nominal function range 5…45 °C Humidity < 80 % Storage –20…60 °C Transport –40…60 °C 7.8 Reference conditions Ambient temperature 25 °C (±3 °C) Relative humidity ≤ 60 % 7.9 Dimensions Width 0.28 m Height 0.73 m Depth 0.50 m Weight (without accessories) 1.814.0010: 14.52 kg 1.814.0020: 15.42 kg 1.814.0030: 13.82 kg 1.814.0110: 18.87 kg 1.814.0120: 19.93 kg 1.814.0130: 16.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 8 Conformity and warranty 8 Conformity and warranty 8.1 Declaration of Conformity This is to certify the conformity to the standard specifications for electrical appliances and accessories, as well as to the standard specifications for security and to system validation issued by the manufacturing company.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 8.2 Warranty (guarantee) EN 61010-2-081 Manufacturer Particular requirements for automatic and semiautomatic laboratory equipment for analysis and other purposes Metrohm Ltd., CH-9101 Herisau/Switzerland Metrohm Ltd. is holder of the SQS certificate ISO 9001:2000 Quality management system for development, production and sales of instruments and accessories for ion analysis. Herisau, 20 February, 2009 8.2 D. Strohm A.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 8.3 8 Conformity and warranty Quality Management Principles Metrohm Ltd. holds the ISO 9001:2000 Certificate, registration number 10872-02, issued by SQS (Swiss Association for Quality and Management Systems). Internal and external audits are carried out periodically to assure that the standards defined by Metrohm’s QM Manual are maintained.
8.3 Quality Management Principles ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ tional Qualification and Performance Verification of the system components or in carrying out the System Validation for the quantitative determination of a substance in a given matrix.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 9 Accessories 9 Accessories Note Subject to change without notice. 9.1 Qty. 1 Scope of delivery 814 USB Sample Processor 2.814.0010 Order no. Description 1.814.0010 814 USB Sample Processor (1T/1P) Highly efficient Sample Processor with one work station and one internal membrane pump. 2 6.1236.020 Sleeve with SGJ 14/12 mm Sleeve with SGJ 14/12 mm and O-ring. Material: PP 5 6.1446.
9.1 Scope of delivery 814 USB Sample Processor 2.814.0010 Qty. 3 Order no. Description 6.1446.010 Stopper Used with Sample Changers Material: Height (mm): Outer diameter (mm): 1 6.1621.000 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ PVDF 19 9.3 Container 10 L As rinsing or waste container in automated systems. Material: PE Width (mm): 265 Height (mm): 400 Volume (mL): 10000 1 6.1805.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 3 9 Accessories Order no. Description 6.1805.420 FEP tubing / M6 / 48 cm With light and kink protection Material: Inner diameter (mm): Length (mm): 1 6.1812.000 PTFE tubing 4/6 mm, 4m Material: Outer diameter (mm): Inner diameter (mm): 1 6.1828.000 6.2053.000 PTFE 6 4 PVDF connection nipple For 6.1621.000 container Material: 1 FEP 2 480 PVDF Cable clip Cable clip for fastening cables and tubes 1 6.2151.
9.1 Scope of delivery 814 USB Sample Processor 2.814.0010 Qty. 1 Order no. Description 6.2621.030 Hexagon key 4 mm Length (mm): 1 6.2621.070 5 mm. Length (mm): ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 73 Hexagon key 5 mm 80 1 6.2621.140 Hexagon key 2.5 mm 3 6.2709.070 Guiding sleeve For fixation of buret and dosing tips in titration heads and electrode holders Material: ETFE Length (mm): 16.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 3 9 Accessories Order no. Description 6.2740.020 Spray nozzle For the fine-spraying of the rinsing solution Material: ETFE Outer diameter (mm): 10 Length (mm): 47 1 6.2751.080 Splash protection Splash protection for single-tower Sample Processors without 786 Swing Head 4 T.240.0102 Ferrite cores Anti-interference adapters 1 6.2122.0x0 Mains cable with C13 line socket IEC-60320-C13 Cable plug according to customer requirements. Switzerland: Type SEV 12 6.2122.
9.2 Scope of delivery 814 USB Sample Processor 2.814.0020 9.2 Qty. 1 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Scope of delivery 814 USB Sample Processor 2.814.0020 Order no. Description 1.814.0020 814 USB Sample Processor (1T/2P) Highly efficient Sample Processor with one work station and two internal membrane pumps. 2 6.1236.020 Sleeve with SGJ 14/12 mm Sleeve with SGJ 14/12 mm and O-ring. Material: PP 5 6.1446.000 SGJ stopper / B-14/(15) Material: Height (mm): SGJ size: 3 6.1446.010 PP 30.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 1 9 Accessories Order no. Description 6.1446.160 Thermometer stopper, B-14/15, oblique insertion To have the inserts of the 6.1458.010 titration head in a sloping position. Material: PTFE Height (mm): 21 Outer diameter (mm): 13 SGJ size: B-14/15 1 6.1543.170 Aspiration tip / M8 thread Aspiration tip to Sample Processors Material: PTFE Length (mm): 198 2 6.1621.000 Container 10 L As rinsing or waste container in automated systems.
9.2 Scope of delivery 814 USB Sample Processor 2.814.0020 Qty. 1 Order no. Description 6.1805.110 FEP tubing / M6 / 80 cm With light and kink protection Material: Inner diameter (mm): Length (mm): 3 6.1805.420 6.1805.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 2 9 Accessories Order no. Description 6.1812.000 PTFE tubing 4/6 mm, 4m Material: Outer diameter (mm): Inner diameter (mm): 1 6.1820.070 PTFE 6 4 Coupler 4/6 mm / M8 inside Extension for aspiration tubings in automated systems. Connects the M8 aspiration tubing directly with the 6.1812.000 PTFE tubing. Material: PTFE 2 6.1828.000 PVDF connection nipple For 6.1621.000 container Material: 1 6.2042.
9.2 Scope of delivery 814 USB Sample Processor 2.814.0020 Qty. 1 Order no. Description 6.2151.000 Cable USB A – mini-DIN 8-pin Controller cable Length (m): 1 6.2621.030 Length (mm): 1 6.2621.070 5 mm. Length (mm): 1 56 ￭￭￭￭￭￭￭￭ 6.2621.140 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1.8 Hexagon key 4 mm 73 Hexagon key 5 mm 80 Hexagon key 2.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 3 9 Accessories Order no. Description 6.2709.070 Guiding sleeve For fixation of buret and dosing tips in titration heads and electrode holders Material: ETFE Length (mm): 16.5 3 6.2740.020 Spray nozzle For the fine-spraying of the rinsing solution Material: ETFE Outer diameter (mm): 10 Length (mm): 47 1 6.2751.080 Splash protection Splash protection for single-tower Sample Processors without 786 Swing Head 4 T.240.
9.3 Scope of delivery 814 USB Sample Processor 2.814.0030 Qty. Order no. ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Description 6.2122.070 1 9.3 Qty. 1 8.814.8001EN 814 USB Sample Processor Manual Scope of delivery 814 USB Sample Processor 2.814.0030 Order no. Description 1.814.0030 814 USB Sample Processor (1T/0P) Highly efficient Sample Processor with one work station and two pump connectors. 2 6.1236.020 Sleeve with SGJ 14/12 mm Sleeve with SGJ 14/12 mm and O-ring. Material: PP 1 6.1805.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 1 Order no. Description 6.2621.030 Hexagon key 4 mm Length (mm): 1 9 Accessories 6.2621.070 5 mm. Length (mm): 73 Hexagon key 5 mm 80 1 6.2621.140 Hexagon key 2.5 mm 3 6.2709.070 Guiding sleeve For fixation of buret and dosing tips in titration heads and electrode holders Material: ETFE Length (mm): 16.
9.4 Scope of delivery 814 USB Sample Processor 2.814.0110 Qty. 1 Order no. Description 6.2751.080 Splash protection ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Splash protection for single-tower Sample Processors without 786 Swing Head 4 T.240.0102 Ferrite cores Anti-interference adapters 1 6.2122.0x0 Mains cable with C13 line socket IEC-60320-C13 Cable plug according to customer requirements. Switzerland: Type SEV 12 6.2122.020 Germany, …: Type CEE(7), VII 6.2122.040 USA, …: Type NEMA/ASA 6.2122.070 1 9.4 Qty.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 4 9 Accessories Order no. Description 6.1236.020 Sleeve with SGJ 14/12 mm Sleeve with SGJ 14/12 mm and O-ring. Material: PP 10 6.1446.000 SGJ stopper / B-14/(15) Material: Height (mm): SGJ size: 6 6.1446.010 PP 30.5 B-14/(15) Stopper Used with Sample Changers Material: Height (mm): Outer diameter (mm): 2 6.1621.000 PVDF 19 9.3 Container 10 L As rinsing or waste container in automated systems.
9.4 Scope of delivery 814 USB Sample Processor 2.814.0110 Qty. 2 Order no. Description 6.1805.110 FEP tubing / M6 / 80 cm With light and kink protection Material: Inner diameter (mm): Length (mm): 6 6.1805.420 6.1812.000 6.1828.000 PTFE 6 4 PVDF connection nipple For 6.1621.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 2 9 Accessories Order no. Description 6.2053.000 Cable clip Cable clip for fastening cables and tubes 1 6.2151.000 Controller cable Length (m): 1 6.2621.030 Length (mm): 1 6.2621.070 5 mm. Length (mm): 814 USB Sample Processor Cable USB A – mini-DIN 8-pin 1.
9.4 Scope of delivery 814 USB Sample Processor 2.814.0110 Qty. Order no. Description 1 6.2621.140 Hexagon key 2.5 mm 6 6.2709.070 Guiding sleeve ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ For fixation of buret and dosing tips in titration heads and electrode holders Material: ETFE Length (mm): 16.5 6 6.2740.020 Spray nozzle For the fine-spraying of the rinsing solution Material: ETFE Outer diameter (mm): 10 Length (mm): 47 1 6.2751.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 4 9 Accessories Order no. Description T.240.0102 Ferrite cores Anti-interference adapters 1 6.2122.0x0 Mains cable with C13 line socket IEC-60320-C13 Cable plug according to customer requirements. Switzerland: Type SEV 12 6.2122.020 Germany, …: Type CEE(7), VII 6.2122.040 USA, …: Type NEMA/ASA 6.2122.070 1 9.5 Qty. 1 8.814.8001EN 814 USB Sample Processor Manual Scope of delivery 814 USB Sample Processor 2.814.0120 Order no. Description 1.814.
9.5 Scope of delivery 814 USB Sample Processor 2.814.0120 Qty. 10 Order no. Description 6.1446.000 SGJ stopper / B-14/(15) Material: Height (mm): SGJ size: 6 6.1446.010 PP 30.5 B-14/(15) Stopper Used with Sample Changers Material: Height (mm): Outer diameter (mm): 2 6.1446.160 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ PVDF 19 9.3 Thermometer stopper, B-14/15, oblique insertion To have the inserts of the 6.1458.010 titration head in a sloping position.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 4 9 Accessories Order no. Description 6.1621.000 Container 10 L As rinsing or waste container in automated systems. Material: PE Width (mm): 265 Height (mm): 400 Volume (mL): 10000 2 6.1805.110 FEP tubing / M6 / 80 cm With light and kink protection Material: Inner diameter (mm): Length (mm): 6 6.1805.
9.5 Scope of delivery 814 USB Sample Processor 2.814.0120 Qty. 2 Order no. Description 6.1805.510 PTFE tubing / M8 / 60 cm With kink protection Material: Inner diameter (mm): Length (mm): 4 6.1812.000 6.1820.070 PTFE 3 600 PTFE tubing 4/6 mm, 4m Material: Outer diameter (mm): Inner diameter (mm): 2 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ PTFE 6 4 Coupler 4/6 mm / M8 inside Extension for aspiration tubings in automated systems. Connects the M8 aspiration tubing directly with the 6.1812.000 PTFE tubing.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 2 9 Accessories Order no. Description 6.2042.020 Buret tip clip (magnetic stirrer) Clip for proper alignment of buret tips, dosing or aspiration tubings using a magnetic stirrer in the titration beaker of a sample changer 2 6.2053.000 Cable clip Cable clip for fastening cables and tubes 1 6.2151.000 Controller cable Length (m): 1 6.2621.030 Length (mm): 1 6.2621.070 5 mm. Length (mm): 814 USB Sample Processor Cable USB A – mini-DIN 8-pin 1.
9.5 Scope of delivery 814 USB Sample Processor 2.814.0120 Qty. Order no. Description 1 6.2621.140 Hexagon key 2.5 mm 6 6.2709.070 Guiding sleeve ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ For fixation of buret and dosing tips in titration heads and electrode holders Material: ETFE Length (mm): 16.5 6 6.2740.020 Spray nozzle For the fine-spraying of the rinsing solution Material: ETFE Outer diameter (mm): 10 Length (mm): 47 1 6.2751.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 4 9 Accessories Order no. Description T.240.0102 Ferrite cores Anti-interference adapters 1 6.2122.0x0 Mains cable with C13 line socket IEC-60320-C13 Cable plug according to customer requirements. Switzerland: Type SEV 12 6.2122.020 Germany, …: Type CEE(7), VII 6.2122.040 USA, …: Type NEMA/ASA 6.2122.070 1 9.6 Qty. 1 8.814.8001EN 814 USB Sample Processor Manual Scope of delivery 814 USB Sample Processor 2.814.0130 Order no. Description 1.814.
9.6 Scope of delivery 814 USB Sample Processor 2.814.0130 Qty. 2 Order no. Description 6.1805.110 FEP tubing / M6 / 80 cm With light and kink protection Material: Inner diameter (mm): Length (mm): 1 6.2151.000 Controller cable Length (m): 1 6.2621.030 Length (mm): 1 6.2621.070 5 mm. Length (mm): 72 ￭￭￭￭￭￭￭￭ ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ FEP 2 800 Cable USB A – mini-DIN 8-pin 1.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 9 Accessories Order no. Description 1 6.2621.140 Hexagon key 2.5 mm 6 6.2709.070 Guiding sleeve For fixation of buret and dosing tips in titration heads and electrode holders Material: ETFE Length (mm): 16.5 1 6.2751.090 Splash protection Splash protection for two-tower Sample Processors without 786 Swing Head 4 T.240.0102 Ferrite cores Anti-interference adapters 1 6.2122.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 9.7 Optional accessories Qty. 1 9.7 Qty. 1 Order no. Description 8.814.8001EN 814 USB Sample Processor Manual Optional accessories Order no. Description 2.741.0010 741 Stirrer Magnetic stirrer for sample changers. The magnetic stirrer is located beneath the sample rack. 1 2.772.0120 772 Pump Unit «aspirate» Peristaltic pump for direct connection to Sample Processors. The «Aspiration» version contains numerous accessories for aspirating off the titrated solution.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 1 9 Accessories Order no. Description 2.802.0020 802 Stirrer Rod stirrer for sample changer and Sample Processor. With 6.1909.020 Propeller stirrer 104 mm and fixed cable. 1 2.823.0020 823 Membrane Pump Unit «aspirate» Membrane pump for direct connection to Sample Processors. The «Aspiration» version contains numerous accessories for aspirating off solutions. 1 2.823.0030 823 Membrane Pump Unit «rinse» Membrane pump for direct connection to Sample Processors.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 9.7 Optional accessories Qty. 1 Order no. Description 2.843.0150 843 Pump Station (peristaltic) - rinse/aspirate for Sample Processors The 843 Pump Station (peristaltic) has two built-in peristaltic pumps. These can be controlled directly from the Sample Processors via pump commands. The rinse/aspirate version is provided with all the accessories needed for automatically emptying the titration beaker and rinsing the titration equipment.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 1 9 Accessories Order no. Description 6.1458.030 KF titration head with 4 x M10 thread With 4 x M10 thread connectors. Material: PTFE Height (mm): 40 Outer diameter (mm): 68 1 6.1458.040 Titration Head, 3 x SGJ14 Titration head for 120 mL beakers. With 3 openings SGJ 14 and 4 openings 6.4 mm, 2 dosing tips included. Suitable for rinsing and aspiration equipment. Material: PTFE 1 6.1458.070 Titration head / 2 x SGJ14 Titration head for 75 mL beakers.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 9.7 Optional accessories Qty. 1 Order no. Description 6.2041.320 Sample rack 16 x 150 mL Sample rack for 16 x 150 mL samples, one-row Material: PVC Outer diameter (mm): 416 Hole diameter (mm): 56 1 6.2041.340 Sample rack 24 x 75 mL Sample rack for 24 x 75 mL samples, one-row. Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 35 1 6.2041.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. 1 9 Accessories Order no. Description 6.2041.460 Sample rack 21 x 100 mL (COD) Sample rack 21 x 100 mL for the determination of COD Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 42 1 6.2041.470 Sample rack 22 x 120 mL Sample rack for 22 x 120 mL samples (6.1459.300), single-row. Material: PP Outer diameter (mm): 420 Inner diameter (mm): 42 1 6.2058.010 Tower extension for Sample Processors Height extension 130 mm for Sample Processors. 1 6.2141.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 9.7 Optional accessories Qty. 1 Order no. Description 6.2711.060 Drip pan for 730/778/814/838 Drip pan for 778, 814, 838 Sample Processors as well as for 730 Sample Changer Material: PVC 1 6.6050.500 Titrando-PC-Control-Software 6.0 PC software for controlling Titrandos, USB Sample Processors, 846 Dosing Interface, 847 USB Lab Link. Simple and intuitive user guidance. Method and data compatible with Touch Control. With freely progammable favorites for fast method access.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Qty. Order no. 9 Accessories Description CFR Part 11 as well as GLP. Dialogue languages: German, English, French, Spanish, Chinese, Korean, Japanese and more. 1 licence. 1 6.6059.202 MagIC Net™ 2.0 Professional CD: 1 licence Professional PC program for controlling intelligent Professional IC systems, Compact IC instruments and their peripherals such as Professional Sample Processors, model 800 Dosinos dosing systems, 771 Compact Interface, etc.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Index Index Numbers/Symbols 685 Dosimat ............................ 27 700 Dosino .............................. 27 741 Stirrer ................................ 23 800 Dosino .............................. 27 801 Stirrer ................................ 28 802 Stirrer ................................ 23 803 Ti Stand ............................. 28 804 Ti Stand ............................. 28 805 Dosimat ............................ 27 A Aspiration equipment ...............
