Full Product Manual

30
ANNEALING PLEXIGLAS
®
Health and Safety Precautions
Annealing Plexiglas
®
acrylic sheet should not result in the
release of harmful concentrations of vapors or gases under the
annealing conditions recommended in this manual. However,
Plexiglas
®
acrylic sheet may release high concentrations of vapors
and monomers if heated to temperatures in excess of 350°F
without adequate ventilation.
The annealing oven should have forced-circulation and should
have bleed and makeup vents, so that the air is changed at least
twice an hour to remove fumes and cement-solvent vapors. Fumes
and cement-solvent vapors should be exhausted to the outdoors.
Parts should be heated to and held at the recommended annealing
temperatures for the recommended times (see Table 6).
Plexiglas
®
acrylic sheet is a combustible thermoplastic material.
Observe fire precautions appropriate for comparable forms of wood
and paper products.
Annealing
Proper annealing is one of the most effective single measures
that can be taken to insure good service from parts made of
Plexiglas
®
acrylic sheet.
Annealing consists of prolonged heating of the acrylic part at
temperatures lower than those used for forming, followed by
slow cooling. Internal stresses set up during fabrication of the
article are reduced or eliminated by this treatment. All edges
should be cut or machined with as little internal stress as possible.
If excessive internal stress is present in the parts to be cemented,
crazing will occur during the cementing process. It may be
necessary to anneal the parts to reduce internal stresses set up
in the parts during fabrication or thermoforming operations.
Annealing results in greater dimensional stability and greater
resistance to crazing. Heat treating also improves the strength
of certain cemented joints.
To obtain the benefits of annealing, the Plexiglas
®
acrylic
sheet parts must be annealed after all fabrication steps, including
polishing, are completed. In addition to annealing after final
finishing, machined parts should be annealed before cementing
to reduce stress due to machining in the cement joint area.
Determination of Best Annealing Temperature
The optimum temperature for annealing any specific part can
best be determined by experimenting with a few samples to find
the maximum temperature at which the part can be heated for
the times indicated in Table 6 without objectionable deformation.
Parts should be annealed at as high a temperature as possible.
Annealing at temperatures lower than those listed in Table 6,
below, will not give effective relief and redistribution of stresses.
Machined Plexiglas
®
acrylic sheet parts that have not been heated
to forming temperature should be annealed with caution in the
higher temperature ranges.
The annealing temperature should be approximately 10°F
below the minimum temperature at which the part shows
deformation of one percent. A greater change indicates that the
part has not been properly formed. The fabrication process
should be carefully reviewed and revised until the parts will
withstand these annealing temperatures. Particular attention
should be given to forming temperatures and conditions because parts
Recommended Annealing Times and Temperatures for Plexiglas
®
Acrylic Sheet
Maximum Thickness
(Inches)
0.060 to 0.177
0.236 to 0.354
0.472 to 0.708
0.944
1.500 to 1.750
2.0
Time* (Hours) to
Heat Mid-Plane
1
2
1
2
3
6
8
221
°
F
(105
°
C)
3
1
2
4
5
6
9
11
* The time required to raise the temperature of the mid-plane to a temperature equal to room temperature plus 99% of the difference between room temperature and annealing temperature.
Notes: (1) Anneal parts at the highest temperature for indicated time. If distortion occurs, try the next lowest temperature.
(2) The cycles given will be satisfactory for most formed parts. For extreme forming, such as 100% biaxial stretching, use lower temperatures.
(3) Air should circulate around each part.
230
°
F
(110
°
C)
1
1
2
2
3
4
7
9
Heating Time (Hours) in Forced-Circulation Air Ovens Maintained at the Indicated
T
emperature for P
arts Made of Plexiglas
®
G and MC Acrylic Sheet
212
°
F
(100
°
C)
7
1
2
8
9
10
13
15
203
°
F
(95
°
C)
24
1
2
25
26
27
30
32
TABLE 6
ACRYLIC SHEET