NIRS™ DA1650 User Manual 6008 1286 / Rev. 8 Copyright 2020 / All rights reserved FOSS Analytical A/S, Nils Foss Allé 1, DK-3400 Hillerød, Denmark Tel Int +45 7010 3370, Fax +45 7010 3371, E-mail info@foss.
NIRS™ DA1650 Information may be changed or updated without notice. The latest version is found at www.foss.dk. Rev. Date of Issue Revised Material 1 2011-05-10 First edition 2 2013-03-25 General update to reflect ISIscan Nova software version 5.2 3 2013-09-13 General update to reflect ISIscan Nova software version 6.0 4 2015-10-21 FOSS address updated 5 2017-06-15 Safety sections moved to seperate manual. General update to reflect Plug and Play installation.
NIRS™ DA1650 Table of Contents 1 Safety .......................................................... 1:1 1.1 General ................................................................... 1:1 1.2 Personal Safety ..................................................... 1:1 1.3 Product Safety ....................................................... 1:2 1.4 Disposal Instructions ............................................ 1:3 1.5 1.5.1 1.5.2 Legal Data ......................................................
NIRS™ DA1650 4.2 4.2.1 4.2.2 4.2.3 4.2.4 Analysis Procedure ................................................ 4:2 Sample Preparation ...................................................... 4:2 Analysing the Sample ................................................... 4:3 Multi-cup Analysis ........................................................ 4:6 Turning off the Analyser .............................................. 4:6 4.3 4.3.1 4.3.2 4.3.3 4.3.4 4.3.5 4.3.6 4.3.7 4.3.8 4.3.9 4.3.10 4.3.11 Care Menu ..
NIRS™ DA1650 1 Safety 1.1 General Please read the user manual carefully and use the instrument as advised. Follow all safety precautions as instructed. Safety Symbols Explanation of safety symbols used in this manual. Symbol Description General hazard. Hot surface. Safety Terminology Explanation of safety terms used in this manual. Term Description Warning Danger to human safety. Caution Danger to product performance/operation. Note Important supplementary information. 1.
NIRS™ DA1650 1.3 Product Safety Caution The instrument is designed and tested for European (CE) compliance. To ensure that this compliance is maintained, connect only CE approved equipment. Connecting equipment that is not CE approved may cause EMC incompatibility and thereby affect the function of the instrument and other equipment. Caution When nothing is connected the sealing caps should be mounted to maintain dust protection.
NIRS™ DA1650 1.4 Disposal Instructions Do not dispose of this electrical device with unsorted household waste. Improper disposal may be harmful to environment and human health. Please refer to your local waste authority for information on return and collection systems in your area. 1.
NIRS™ DA1650 • the product has not in any other ways been handled contrary to ordinary practice • only software authorised by FOSS has been installed on any product PC • any external product PC has complied with the recommendations of the FOSS representative • computer games have not been played on the PC, including any games preinstalled together with the operating system.
NIRS™ DA1650 2 Introduction 2.1 General NIRS™ DA1650 is a robust, simple-to-use and accurate near-infrared analyzer that is based on diode array technology. NIRS DA1650 is a robust instrument that can be used in a laboratory or at-line environments. The user interface is designed for simple daily routine operation. Measurements are simple to perform and results are delivered in minutes. The analyzer is easy to move around and can be placed close to the production line.
NIRS™ DA1650 Fig. 2:2Rear view of NIRS DA1650 1 2 3 2:2 On/Off switch Fuse holder Power cable connection 4 5 Ethernet connection USB connection User Manual 6008 1286 / Rev.
NIRS™ DA1650 2.2 Principle of Operation A sample, ground or unground, is placed in a sample cup which is placed in the instrument. By means of a motor, the cup is turned so that multiple parts of the sample is scanned. This multipoint reflectance measurement allows for an accurate analysis of the sample. For inhomogeneous samples like pellets it is crucial with a multipoint measurement. Fig. 2:3Sample cup in instrument 2.3 Sample Cups 2.3.
NIRS™ DA1650 Fig. 2:4Sample cups A B 2.3.2 Small cup Small cup holder C Large cup Radio Frequency Identification System Radio Frequency Identification (RFID) is a method used by the NIRS DA1650 for identifying each individual sample cup. There is a small RFID chip in each cup with CupType information and a unique CupID. The CupType information can be used to ensure that the correct Cup Type is used for each measurement.
NIRS™ DA1650 2.3.3 Other Cups and Accessories Fig. 2:5Other cups and accessories A B C Large cup extension Slurry cup Lid for small cup User Manual 6008 1286 / Rev.
NIRS™ DA1650 Large Cup Extension The "large cup extension" fits on the bottom part of the Large sample cup. It can be used when a larger sample volume is required in order to scan a representative portion of the sample. Slurry Cup The best choice for samples that tends to stick to the cup. Also the preferred choice for samples warmer than 50 °C. Should only be used for homogenous samples. Petri Dish Holders For wet, sticky or otherwise unpleasant samples. Can be used with plastic or glass petri dishes.
NIRS™ DA1650 2.4 NIRS DA1650 Software NIRS DA1650 is operated by two separate software programs: • ISIscan Nova • Mosaic Solo This User Manual describes the main features and work flows for routine operation in ISIscan Nova software and some of the FossManager software which is used for configurations and setup. In both softwares there are built-in help files which can give further information on specific details. 2.4.1 ISIscan Nova ISIscan Nova is the operating software for the NIRS DA1650.
NIRS™ DA1650 The two scenarios are shown below. Fig. 2:8FossManager - Solo setup • Instrument configurations managed locally from an external PC running FossManager software. • Routine Operator operates NIRS DA1650 via ISIscan Nova software via the built-in touch screen. Fig. 2:9FossManager - Network setup • Instrument configurations managed remotely by the Network manager using FossManager software. • Routine Operator operates the NIRS DA1650 via ISIscan Nova software via the built-in touch screen.
NIRS™ DA1650 2.4.3 Routine Operation Software The NIRS DA1650 analyzer is supplied with software to support all the necessary functions and features to operate the system on a daily basis. Touch Screen Display Fig.
NIRS™ DA1650 Sample registration values These can be lists or free text fields. Lists are indicated with an arrow and free text fields with a keyboard . A star will indicate if the field is mandatory and has to be filled out. Once the sample is synchronised to the FossConnect server it can no . longer be edited, which is indicated with a small padlock icon Start/Stop analysis Press to start analysis. Once analysis has been initiated the button turns into a stop button.
NIRS™ DA1650 Care Menu The Care View Menu contains features not related to routine analysis. They are described in chapter 4 and you need to go through some of them during installation to ensure your instrument is configured correctly. This is also the view you use for some regular or ad hoc activities (e.g. database backup, instrument diagnostics, FossManager synchronisations for Networked instruments). Fig. 2:11 Fig. 2:12 User Manual 6008 1286 / Rev.
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NIRS™ DA1650 3 Installation 3.1 Site Preparation A Site Preparation Check List is available from your FOSS representative. This document describes the necessary arrangements to be carried out or tested prior to installation. If this has not been done in advance the check list items should be considered during installation to ensure that the instrument is installed properly. 3.2 Unpacking and Checking Unpack the NIRS DA1650 and its accessories with care. Save all packing material for later use.
NIRS™ DA1650 3.5 PC connection for Mosaic Solo Instruments are configured with Foss standard setup and purchased calibrations at the time of delivery. So a PC only needs to be connected if changes from the standard setup is required. Connect the instrument to the PC in a way that is suitable for the current installation. 3.5.1 Installation of Mosaic Solo on external PC For carrying out Configurations and other tasks in Mosaic Solo (when running the instrument in Solo mode, see 2.
NIRS™ DA1650 Fig. 3:2 You can use the Computer name if the instrument is connected to an office network with DHCP and name server otherwise you need to use the IP address of the instrument. A log-in is required to access the internal folder of the NIRS DA1650. • Username: administrator • Password: ms2361 4. Press OK. User Manual 6008 1286 / Rev.
NIRS™ DA1650 Fig. 3:3 5. You will now see a shared folder in the NIRS DA1650. Open the folder "DA1650Setup.exe". Fig. 3:4 6. 3:4 Start installation via "setup.exe". User Manual 6008 1286 / Rev.
NIRS™ DA1650 Fig. 3:5 7. Click Run. Fig. 3:6 Depending on whether you have had Mosaic installed before or not on this PC, you will see a number of components being installed. At this stage you might get a request to install Crystal Reports Runtime. This happens if you don’t have Crystal Reports installed or if you have an older version on your computer. 8. Click Accept. User Manual 6008 1286 / Rev.
NIRS™ DA1650 Fig. 3:7 9. 3:6 Press Install to start installation User Manual 6008 1286 / Rev.
NIRS™ DA1650 Fig. 3:8 The installation takes five to fifteen minutes depending on whether you need to have the Crystal Report Runtime installed or not. Fig. 3:9 After the installation, the Mosaic Solo will start automatically. It can also be started via the icon which now should be on your PC desktop. Fig. 3:10 User Manual 6008 1286 / Rev.
NIRS™ DA1650 If installation of Mosic Solo fails In some cases, Windows 10 PC's are not able to connect to Windows Embedded 2009 instrument as the DA1650 / MeatScan / Olivia / Dairy. When this happens SMBv1 needs to be enabled. This is procedure to enable the SMBv1 feature. 1. Navigate to: Control Panel\All Control Panel Items\Programs and Features. 2. Select ‘Turn Windows feature on or off’. Fig. 3:11 3. When "Windows Features" pops up, scroll down and check the "SMB 1.
NIRS™ DA1650 3.5.2 Via Local Area Network Connect instrument to a LAN with the enclosed network cable and connect the PC to the same LAN with a standard network cable (not included with instrument). Since ISIscan Nova can see other instruments connected to the same LAN it is important that the correct instrument serial number is entered (when prompted) first time ISIscan Nova is started. If the LAN is connected to the Internet, no other connections are needed to synchronise with FossConnect server. 3.5.
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NIRS™ DA1650 4 Operating Instructions 4.1 Routine Start-up 1. Turn on the analyzer by pressing the On/Off switch placed at the rear of the instrument. The analyser will now start up, initializing the software. This will take several minutes. Once the software is ready, the instrument will go through the start-up tests. The instrument is ready for analysis when the start-up test has succeeded. Fig.
NIRS™ DA1650 The most likely reason for selftest to fail is that the instrument is not warmed up properly. Please wait 5-10 minutes and repeat the selftest by going to the Care menu and select Instrument Diagnostics. If the problem persists, please contact your local FOSS representative and also forward the diagnostic report to them. You can still carry out analysis but every result will be highlighted in yellow, with a warning stating that the Startup test was not completed.
NIRS™ DA1650 4.2.2 Analysing the Sample 1. Instrument should be warmed up 30 minutes prior to first analysis. 2. Choose the appropriate sample cup for the sample. See chapter 2 for information about the different cup types. 3. Carefully prepare your sample and fill the sample cup all way up. Sample types that tend to form voids if simply poured in should be compressed using the back of a spoon or similar. 4. Place the filled sample cup in the sample compartment and close the lid. Fig. 4:4 5.
NIRS™ DA1650 Products are installed and configured in FossManager. (Please refer to the Installation Guide for details.) 6. Select a product and press Start to initiate the analysis sequence. Fig. 4:6 The specific cup to use with the selected product can be indicated along with the product name. (This cup type indication can be enabled/disabled in the Operation profile in FossManager.) 7. Register sample information by clicking in the ID fields on the right hand side.
NIRS™ DA1650 8. A progress indicator shows sample analysis progress. Fig. 4:8 9. Once the analysis is complete, the result is displayed and the lid can be opened. Fig. 4:9 10. Previous results can be viewed by scrolling backward/forward with the arrows in top right corner. 11. The results are presented on the screen and can be printed/reported via the Reports view. (Configuration of manual reports to be available in the Reports view is done in FossManager under Instrument Settings.
NIRS™ DA1650 4.2.3 Multi-cup Analysis For some sample types it is desired to split a larger sample volume into sub-samples and report the results as the average of these sub-samples. This is support in NIRS DA1650 via the Multi-cup analysis. In the Operation Profile in FossManager you set the number of sub-samples (repetitions) for the product in question. In ISIscan Nova this is indicated together with the product name. Fig.
NIRS™ DA1650 4.3 Care Menu The Care view contains features not related to routine analysis. They are described on the following pages and you need to go through some of them during installation to ensure your instrument is configured correctly. This is also the view you use for some regular or ad-hoc activities (e.g. database backup, instrument diagnostics, FossManager synchronisations for Networked instruments). Fig. 4:12 Fig. 4:13 User Manual 6008 1286 / Rev.
NIRS™ DA1650 4.3.1 FossManager Synchronisation This view looks different when software is installed in Network mode or Solo mode (see section 2.4.2 local configuration and the Installation Guide for information about the two modes). FossManager synchronisation is only applicable if your instrument is installed in Network mode. This button is grayed out if the instrument is installed in Solo mode. (See section 2.4 for information about Network and Solo modes.
NIRS™ DA1650 Fig. 4:15 4.3.2 Instrument Diagnostics Running Instrument Diagnostics from the Care menu will carry out the same tests and with the same test limits as during the Start Up test. After the Instrument Diagnostics is completed, you can create and store the Diagnostic Report in the same way as after the Start up test (see section 4.1 Routine Start-up). 4.3.
NIRS™ DA1650 Fig. 4:16 4.3.4 Instrument Calibration Instrument Calibration of NIRS DA1650 is a task normally carried out by a FOSS representative at the time of installation and/or at service or Preventive Maintenance visits. NIRS DA1650 is using DDA technology (diode array) which is very stable over time and insensitive against e.g. vibrations. The instrument calibration performed prior to delivery or at installation will therefore last a long time.
NIRS™ DA1650 Intensity Correction 1. Place the ERC tool in the instrument with the help of the small cup holder. Insert the ERC USB key in the USB port on the back panel. 2. Select Intensity Correction and press Calibrate. Fig. 4:17 3. Running instrument calibration requires you to enter the 4-digit password "1234" (preventing un-intentional start of the calibration sequence). Fig. 4:18 4. If the ERC key is not properly connected to the instrument, a message will appear. Fig. 4:19 5.
NIRS™ DA1650 Instrument Calibration 1. Place the EWC tool in the instrument with the help of the small cup holder and close the lid. 2. Insert the EWC USB key in the USB port on the back panel. 3. Select Instrument Calibration and press Calibrate. Fig. 4:20 4. Running instrument calibration requires you to enter the 4-digit password "1234" (preventing un-intentional start of the calibration sequence). Fig. 4:21 5. If the EWC key is not properly connected to the instrument, a message will appear.
NIRS™ DA1650 4.3.5 Maintenance Maintenance view for: • Manual backup of database (for automatic backup of database, see section 4.3.11 Configuration) • Restore of existing database backup • Deletion of samples Fig. 4:23 Backup Backup will create a backup file, e.g. DA1650_sn26090_v6.0_D20130325T115035 (name includes serial number, date and time) and save this to the destination as set in Configuration view (4.3.11). Fig. 4:24Example of database backup file User Manual 6008 1286 / Rev.
NIRS™ DA1650 Fig. 4:25 Fig. 4:26 Fig. 4:27 4:14 User Manual 6008 1286 / Rev.
NIRS™ DA1650 Restore Restore will open a view where you are asked to browse to the backup file you want to restore. 1. Press Restore. Fig. 4:28 Note: Restoring a database will erase all existing data and configurations from your ISIscan Nova installation. 2. Press Yes to continue. Fig. 4:29 User Manual 6008 1286 / Rev.
NIRS™ DA1650 Fig. 4:30 Delete now Delete now is a function for manual deletion of samples older than the date specified in the text. This date is determined by settings in FossManager. (Default setting in FossManager is "older than 60 days".) Pressing Delete now will prompt you for the PIN code "1234" (to avoide unintentional deletion). Fig. 4:31 4.3.6 Shut Down Press SHUT DOWN to shut down the instrument. 4:16 User Manual 6008 1286 / Rev.
NIRS™ DA1650 4.3.7 Upgrade NIRS DA1650 is delivered with the latest available software version (ISIscan Nova) If at a later stage the software needs upgrading to a later version and/or configuration, this requires that a USB with the relevant software package is connected to the instrument. The Upgrade procedure can then be initiated locally on-site from the Care view in ISIscan Nova. Please request the latest version of this USB and SW package when needed for onsite upgrades.
NIRS™ DA1650 4.3.8 Instrument Information Instrument information contains e.g. serial number, software versions, IP-address etc. If you need to report a problem it is recommended that you include this type of info when contacting the FOSS representative. Fig. 4:33Example of instrument information 4.3.9 Remote Support Remote Support is a tool to set up a TeamViewer session to enable a remote support session with a support engineer. An internet connection is required.
NIRS™ DA1650 4.3.10 Export Logs Export Logs is a command for collecting internal log-files from ISIscan Nova and Mosaic Solo . Fig. 4:34 Typically these log-files contain detailed and traceable information about the instruments operation but they do not contain any sample data or results. This command is used when log-files are requested by your FOSS representative e.g. for support issues.
NIRS™ DA1650 4.3.11 Configuration The Configuration view contains settings which normally are done at time of installation but they can also be edited afterwards. 1. Press Configuration. Fig. 4:35 On the FossManager Configuration tab you enter the Address and Port number for the FossManager Network server to be used for this particular instrument. This information will be provided to you by the Network manager or the FOSS representative at time of installation.
NIRS™ DA1650 If the correct Address/Port number is entered and interconnection is OK, you will get the message “Connection to FossConnect server was successful” next to tbe button. Fig. 4:37 Fig. 4:38 On the Reporting tab you set the paths for Manual/Automatic reports and for LIMS export. If the NIRS DA1650 is not connected to a local network, then the recommendation is to set these paths to point to a USB memory connected to the instrument, allowing easy access to the reports and exported files.
NIRS™ DA1650 Fig. 4:39 4.4 Check Samples 4.4.1 Check Sample This refers to the empty check sample cell which is filled with a local sample and used together with prediction models suitable for that sample type. For info about the artificial FOSS Check Sample please see section 4.4.2 FOSS Check Sample. A Check Sample (or Control Sample) is measured on a regular basis to validate the stability of the analyzer and everything around it that affects its performance (environment etc.).
NIRS™ DA1650 Before running the check sample you must create a check sample Product in FossManager. 1. Import the prediction model(s) you intend to use for your check sample and link a Parameter profile. (Create a new Parameter profile if needed.) 2. Create an Operation profile with Cup Type = “Check sample (sealable)” and name it e.g. "Check Sample" Fig. 4:40 3. • • • • Create a Product and call it e.g. Check Sample.
NIRS™ DA1650 • Absolute limits • Relative limits with a defined target • Relative limits without a defined target 4:24 User Manual 6008 1286 / Rev.
NIRS™ DA1650 Absolute limits If Absolute limits are defined in FossManager for your check sample then the target has no meaning. The check sample test will give a Warning or Error based on the defined absolute limits. Example: • Error Low: 8 %; Warning Low: 9.5 %; Warning High: 12.5 % ; Error High: 14% Running a check sample definition is then not necessary as no target value is needed.
NIRS™ DA1650 4. Press Start and enter pin code “1234” to run the check sample definition. Fig. 4:43 5. The check sample will now go through a series of analysis. ISIscan Nova may ask you for a Sample number (depending on settings in Operation profile. A Sample number is not required, but if you have more than one check sample it could be wise to enter the Serial number of the check sample in this field for future reference. 6.
NIRS™ DA1650 The sample inside the check sample cell may have changed over time and the proper action would then be to either replace the sample and/or to run a new check sample definition to re-define the target values or even review the limits in FossManager. If the check sample is deemed to be OK and fresh then running the Instrument Diagnostics (from Care view) may give you an indication if something has changed inside the instrument.
NIRS™ DA1650 3. • • • • Create a Product and call it e.g. Check Sample FOSS. In the different tabs you: Link the operation profile you just created above Link the prediction model(s) you imported above Add the Instrument Group where the instrument in question is registered. Set check sample limits for this new product. (See separate section below.) Fig. 4:46 4. If you are on a FossManager Network you can now set up an Update session in order to download the Check Sample product to the instrument(s).
NIRS™ DA1650 Example: Fig. 4:47 Running a Check Sample definition (ISIscan Nova) The check sample definition will every time it is performed re-define the target for the check sample but it will not change the limit-settings (these can only be changed in FossManager). 1. Select the check sample product and tick the box on the right hand side so the Product name changes to "Check Sample (Definition)" Fig. 4:48 2. Place the check sample in the instrument using the small cup holder. 3. Close the lid.
NIRS™ DA1650 4. Press Start and enter pin code “1234” to run the check sample definition. Fig. 4:50 5. The check sample will now go through a series of analysis. ISIscan Nova may ask you for a Sample number (depending on settings in Operation profile. A Sample number is not required, but if you have more than one check sample it could be wise to enter the Serial number of the check sample in this field for future reference. 6. Result for the check sample test is displayed after analysis.
NIRS™ DA1650 5 Maintenance A NIRS DA1650 requires little maintenance. The instrument enclosure is sealed to prevent contamination of critical modules, which keeps maintenance to a minimum. DO NOT attempt to open the instrument enclosure. There are no user-serviceable parts inside the instrument enclosure. Damage is not covered under warranty. 5.1 Cleaning the Instrument Wipe the instrument cabinet with a moist cloth on a regular basis.
NIRS™ DA1650 5.4 Replacement of Lamp The instrument should be well cleaned before replacement of the lamp to prevent dust from damaging the reflector. The replacement should be performed in a clean environment. Warning The lamp module can be very warm if the operating temperature is high. Cotton gloves must be used when replacing the lamp to avoid burn injuries. Caution Do not touch the lamp glass or reflector or let any rough surface come into contact with the lamp glass.
NIRS™ DA1650 3. Carefully turn the lamp assembly and remove it from the instrument. 4. Use the supplied flat bladed screwdriver to loosen the two screws holding the lamp cables. Fig. 5:2Removing lamp from cover plate 5. Fit the new lamp and assemble in reverse order. Note: Push the cables in when you fit the lamp assembly back in place. Make sure the cables are not squeezed. 5.
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NIRS™ DA1650 6 Troubleshooting 6.1 General The NIRS DA1650 analyzer is designed to be a dependable, trouble-free instrument with many years of use. In spite of the rugged design, problems may arise that require attention. There are no user-serviceable parts inside the instrument enclosure except the lamp. Because of this design, we emphasize that under no circumstances should the user attempt to open the instrument cabinet and service any part besides the lamp.
NIRS™ DA1650 6.2 Recommended Actions Fault Action Check incoming power The instrument doesn't start Check the Power Supply Check the fuse Unfamiliar internal noise Restart the instrument. Turn off if problem persists Display is black Contact your FOSS representative Touch screen doesn't work Contact your FOSS representative 6:2 User Manual 6008 1286 / Rev.
NIRS™ DA1650 6.3 Error Messages Fault Action 1 Too much light - Sample too light Check sample cup 2 Too little light - Sample too dark Check sample cup 3 Internal error: Inconsistent measurements Please restart instrument. Contact your FOSS representative if problem persists 4 Internal error: Invalid measurement settings Contact your network administrator for a new update session 5 Instrument temperature is too low Re-start instrument.
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NIRS™ DA1650 7 Parts, Accessories and Consumables See the Owner’s Guide. User Manual 6008 1286 / Rev.
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NIRS™ DA1650 8 Technical Specifications 8.1 Technical Data NIRS™ DA1650 Dimensions (W x D x H) 230 x 530 x 280 mm Weight 16 kg Fuse 6.3 A Power consumption 70 VA Noise level < 70 dB(A) Degree of protection IP 65 8.
NIRS™ DA1650 8.3 Prformance Data NIRS™ DA1650 Measurement mode Reflectance or transflectance (for liquids) Wavelength range 1100-1650 nm Detector 256 pixel InGaAs diode array Optical bandwidth 10.44 ±0.5 nm Number of data points 1100 Absorbance range Up to 2 AU Number of sub-samples Default: 7 for analysis in Small Cup; 8 for analysis in Large Cup (can be set via FossManager) Analysis time 1 minute for 8 sub-samples Self-test 30 minutes at room temperature Spectral resolution 0.
